Journal
GREEN CHEMISTRY
Volume 20, Issue 16, Pages 3696-3699Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c8gc01766b
Keywords
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Funding
- Natural Sciences Foundation of Zhejiang Province [LY18H300001]
- National Natural Science Foundation of China [81473074, 81673291, 81602959]
- Osteoporosis & Breast Cancer Research Center, USA
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A one-pot, catalyst-free, three-component sequential double-annulation from amine alcohols, glyoxal monohydrates and KSCN underwent imine formation/intramolecular cyclization/[3 + 2] cycloaddition. This tandem and green reaction offered [1,3] oxazine N-fused imidazole-2-thiones in a mild condition, with a very short reaction time, wide variation in functional groups, high efficacy on the gram-large scale and followed group-assisted purification chemistry work-up.
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