Journal
RSC ADVANCES
Volume 5, Issue 44, Pages 34517-34524Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c5ra05305f
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Funding
- MEC [MAT2011-23593]
- Junta de Andalucia [JA FQM 06090]
- CSIC [201460E005]
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The aim of this study was to find a surfactant-free method for the synthesis of uniform Eu: LuPO4 nanophosphors which are able to form stable colloidal suspensions in aqueous media. Uniform, ovoid Eu-doped LuPO4 fluorescent nanoparticles were obtained after aging for 30 minutes at 180 degrees C a butylene glycol solution containing, exclusively, lutetium acetate, europium acetate and H3PO4. XRD and digital diffraction patterns of HRTEM images suggested that the particles were single crystalline in nature with the c-axis of the unit cell parallel to the long particle axis. The luminescence study revealed that the optimum doping level was 5 molar%. The latter particles (85 nm x 40 nm dimensions) were functionalized with polyacrylic acid and their colloidal stability in two different biological buffers was demonstrated to persist for at least 15 days.
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