Journal
EUROPEAN JOURNAL OF ORGANIC CHEMISTRY
Volume 2018, Issue 13, Pages 1533-1537Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/ejoc.201800011
Keywords
Fused-ring systems; Synthetic methods; Photochemistry; Photoredox catalysis; Radicals; Intramolecular cyclization
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Funding
- University Grants Commission (UGC), New Delhi
- Department of Science & Technology (DST), New Delhi [EMR/2016/006975]
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A mild and efficient photocatalytic protocol for the synthesis of the phenanthrene scaffold has been devised. The reaction involves intramolecular cyclization of -keto vinyl radicals generated from -bromochalcones under visible light photoredox catalyzed (VLPC) conditions. The high product yields, wide substrate scope, and complete regioselectivity are notable attributes of the reaction.
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