Journal
RSC ADVANCES
Volume 5, Issue 105, Pages 86056-86060Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c5ra18471a
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Funding
- National Natural Science Foundation of China [21076035, 20972022]
- Program for New Century Excellent Talents in University [NCET-11-0053]
- Fundamental Research Funds for the Central Universities [DUT13ZD202]
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A zinc chloride catalyzed tandem 1,5-hydride shift/cyclization process to form spiropyrazolone terahydroquinoline derivatives is developed. A series of new spiropyrazolone derivatives were obtained in good to high yields with good to excellent diastereoselectivities (up to 95% yield, >95 : 5 dr). Additionally, the spiropyrazolone derivatives could be converted into the corresponding novel spriopyrazolines.
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