Journal
COLLOIDS AND SURFACES A-PHYSICOCHEMICAL AND ENGINEERING ASPECTS
Volume 538, Issue -, Pages 451-459Publisher
ELSEVIER SCIENCE BV
DOI: 10.1016/j.colsurfa.2017.11.037
Keywords
Nickel cobaltite; Aerogels; Nanocomposite; Hybrid capacitor
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Funding
- Basic Research Laboratory Program through the National Research Foundation (NRF) - Ministry of Science, ICT&Future Planning of Republic of Korea [2014R1A4A1008140]
- Basic Research Program through the National Research Foundation of Korea (KRF) - Ministry of Education [2017R1D1A1B03034626]
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A facile sol-gel route is developed to build mesoporous 3D NiCo2O4/MWCNT nanocomposite aerogels. The crystal structure, surface morphology and electrochemical performance of the aerogel composites are investigated by X-ray diffraction (XRD), Field-emission scanning electrochemical spectroscopy (FE-SEM) and electrochemical measurements. The effects of MWCNT concentration on the capacitance performance of MWCNT/NiCo2O4 aerogels are studied. It is found that the NiCo2O4/ MWCNT nanocomposite aerogels with MWCNTs similar to 2.1 wt% reach the maximum specific capacitance of up to 1010 F g(-1) at a discharge current density of 0.1 A g(-1) with excellent cyclic stability. Further, these materials are applied for solid-state asymmetric supercapacitors and show higher areal capacitance value (471.8 mF cm(-2)) at a current density of 5 mA cm(-2) with good cycle stability and glowing red LED for 3mins. The superior electrochemical performance is due to the mesoporous structure and well-connected metal nanoparticles with MWCNT in the nanocomposite aerogels, which can provide more active sites to enhance the electrochemical performance of the device.
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