Journal
CHEMICAL COMMUNICATIONS
Volume 54, Issue 60, Pages 8355-8358Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c8cc04487b
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Funding
- EPSRC [EP/L019655/1] Funding Source: UKRI
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Mechanochemistry enabled the selective synthesis of the recherche orange polymorph of Wilkinson's catalyst [RhCl(PPh3)(3)]. The mechanochemically prepared Rh-complex catalysed the solvent-free dehydrogenation of Me2NHBH3 in a ball mill. The in situ-generated hydrogen (H-2) could be utilised for Rh-catalysed hydrogenation reactions by ball milling.
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