Journal
CHEMICAL COMMUNICATIONS
Volume 54, Issue 26, Pages 3258-3261Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c8cc01446a
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- Czech Academy of Sciences (Research Plan) [RVO: 61388963]
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A rhodium-catalyzed transannulation via ring-opening of N-(per)fluoroalkyl-substituted 1,2,3-triazoles followed by cycloaddition with different nitriles, enol ethers, isocyanates and silyl ketene acetals under microwave heating provided a highly efficient route to previously unreported N-(per) fluoroalkyl-substituted imidazoles, pyrroles, imidazolones and pyrrolones, respectively. These reactions were found to be applicable to the synthesis of a variety of 5-membered heterocycles bearing different (per) fluoroalkyl substituents aswell as both electron-donating and electron-withdrawing groups attached to the heterocyclic core.
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