Journal
BOLETIN DE LA SOCIEDAD ESPANOLA DE CERAMICA Y VIDRIO
Volume 57, Issue 5, Pages 213-220Publisher
ELSEVIER SCIENCE BV
DOI: 10.1016/j.bsecv.2018.04.004
Keywords
Sol-gel; Particle size; Milling; beta-TCP; Powders
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Funding
- UNAM-DGAPA-PAPIME [PE104318]
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beta-Tricalcium phosphate (beta-TCP) is one of the most investigated calcium phosphates to be used in bone tissue regeneration. Nowadays, beta-TCP has been synthetized by different methods that allow obtaining different morphologies with chemical compositions similar to the bone tissue, broadening the possibilities of use. In this work, beta-TCP powders were obtained using two different routes: mechanosynthesis and sol-gel. Results shown that both methods had significant effects on morphology and size particle of the obtained powders. The average size particles obtained using mechanosynthesis at 24 and 12 h of milling time were 1000 and 170 nm, respectively. The average size particles of the powders fabricated using sol-gel was 350 nm, and the average powder particle size of the sigma reagent was 1450 nm. Besides, sol-gel and sigma reagent powders were observed residual phases, instead mechanosynthesis shown only tricalcium phosphate beta phase. The formation of agglomerates with different sizes was observed in both methods by sol-gel and mechanosynthesis. (C) 2018 SECV. Published by Elsevier Espana, S.L.U.
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