Journal
PHYSICAL REVIEW B
Volume 93, Issue 5, Pages -Publisher
AMER PHYSICAL SOC
DOI: 10.1103/PhysRevB.93.054202
Keywords
-
Funding
- Czech Science Foundation [15-04121S]
- European Community [226716]
Ask authors/readers for more resources
The method for three-dimensional imaging with an atomic resolution, based on the measurement of resonant scattering of x rays, is presented and tested on a nanoscale-range occupational ordering of niobium and magnesium ions in the lead magnesium niobate (PbMg1/3Nb2/3O3) single crystal. X-ray diffuse scattering experiments performed at two wavelengths close to the absorption edge of niobium allowed us to record two 1024 x 1024 x 1024 data sets of scattering intensities covering densely a large volume of the reciprocal space (up to Q(max) = 8.5 angstrom(-1), with steps smaller than delta Q = 0.05 angstrom(-1)). It is demonstrated that the anomalous part of the scattering intensity, including both discrete diffraction spots and diffuse scattering, can be employed to reconstruct the local atomic environment around the niobium cation up to the distance of several nanometers.
Authors
I am an author on this paper
Click your name to claim this paper and add it to your profile.
Reviews
Recommended
No Data Available