Journal
ANGEWANDTE CHEMIE-INTERNATIONAL EDITION
Volume 57, Issue 18, Pages 5124-5128Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/anie.201801109
Keywords
aza-Heck reaction; cascade reactions; N-heterocycles; palladium
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Funding
- EPSRC [EP/M506473/1]
- FAPESP [2016/00422-0]
- AstraZeneca
- Biotechnology and Biological Sciences Research Council [BB/F011539/1] Funding Source: researchfish
- Engineering and Physical Sciences Research Council [EP/K03927X/1, 1627995, EP/L011999/1] Funding Source: researchfish
- BBSRC [BB/F011539/1] Funding Source: UKRI
- EPSRC [EP/L011999/1, EP/K03927X/1] Funding Source: UKRI
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Ligand-enabled aza-Heck cyclizations and cascades of N-(pentafluorobenzoyloxy)carbamates are described. These studies encompass the first examples of efficient non-biased 6-exo aza-Heck cyclizations. The methodology provides direct and flexible access to carbamate protected pyrrolidines and piperidines.
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