Journal
RSC ADVANCES
Volume 6, Issue 68, Pages 63660-63666Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c6ra10097j
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Funding
- Consejo Nacional de Ciencia y Tecnologia, CONACyT [181448]
- SNI (Sistema Nacional de Investigadores)
- CONACyT
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Cu(Al)O mixed oxides, which are obtained by the calcination of Cu-Al layered double hydroxide (LDH), promote the formation of 1,2,3-triazoles from an alkyne-azide cycloaddition reaction (Huisgen-type reaction) with excellent yields using an EtOH-H2O mixture as the solvent under microwave heating. The yield of the reaction is the result of both heterogeneous and homogeneous catalytic processes, as a consequence of capturing Cu(II) from the material by sodium ascorbate. Although the appropriate reaction conditions were employed (EtOH-H2O, 80 degrees C, MW, 10 min), the reconstruction of LDH by the so-called memory effect was not observed.
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