Journal
ORGANIC CHEMISTRY FRONTIERS
Volume 4, Issue 11, Pages 2175-2178Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c7qo00604g
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Funding
- National Natural Science Foundation of China [21202092]
- Startup Foundation of China Three Gorges University [KJ2012B080, KJ2014H008]
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A practical one-pot synthesis of tetrahydroquinoxalines from readily available 2-amino(nitro) anilines and 1,2-dicarbonyl compounds mediated by diboronic acid with water as both a solvent and a hydrogen donor under metal-free conditions has been discovered. The deuterium labeling experiments with D2O were also performed to demonstrate that water acts as the hydrogen donor.
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