Journal
ORGANIC CHEMISTRY FRONTIERS
Volume 4, Issue 11, Pages 2226-2229Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c7qo00595d
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Funding
- National Natural Science Foundation of China [21372044]
- Fuzhou University [022494]
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A nucleophilic trifluorovinylation of organothiocyanates catalyzed by tetrabutylammonium fluoride has been developed. In this transformation, a variety of aryl and alkyl thiocyanates reacted with trifluorovinyl trimethylsilane to afford 1,2,2-trifluorovinyl sulphides. This transformation was extended to organic selenocyanates to afford 1,2,2-trifluorovinyl selenides. The presented methodology is simple and mild, and can also be used to prepare 1,2,2-trifluorovinyl sulphoxides from organothiocyanates.
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