4.3 Article

Approximating the near-edge mass absorption coefficients for Ni using an ultra-thin bimetal foil

Journal

JOURNAL OF APPLIED CRYSTALLOGRAPHY
Volume 50, Issue -, Pages 1-13

Publisher

INT UNION CRYSTALLOGRAPHY
DOI: 10.1107/S1600576716017544

Keywords

mass absorption coefficients; nickel; titanium; absorption; ultra-thin foils; Ni K edge

Funding

  1. US Department of Energy, Office of Biological and Environmental Research [DE-AC02-06CH11357]

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In an effort to improve the characteristics of a fluorescing metal-foil-based beam position monitor, a new bimetal ultra-thin (0.98/0.67 mu m) Ti-Ni foil was introduced to replace an existing single-element ultra-thin 0.5 mu m thick Cr foil. During characterization it was determined that absorption measurements on the bimetal foil could be used to fit the Ni mass absorption coefficients accurately in the vicinity of the Ni K edge. Comparison with experimental results from the literature demonstrated that the fitting procedure produced coefficients with uncertainties of the order of +/- 1%. Once determined, these fit coefficients allowed the thickness of an independently mounted 8 mm thick Ni foil to be computed from absorption measurements instead of relying on a tool-based measurement of the foil thickness. Using the 8 mm thick foil, a continuous map of Ni mass absorption coefficients was produced at 1 eV resolution throughout the near-edge region. This high-resolution map marks a significant improvement over the existing NIST XCOM or FFAST database mass absorption coefficients, which have estimated errors of 10-20% for the near-edge region.

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