Journal
CURRENT MICROWAVE CHEMISTRY
Volume 3, Issue 1, Pages 14-23Publisher
BENTHAM SCIENCE PUBL LTD
DOI: 10.2174/2213335602666150119221147
Keywords
Alkynes; azides; catalysis; 1,3-dipolar; click chemistry; copper; cycloaddition; green chemistry; heterocycles; microwave; 1,2,3-triazoles; nitrogen compounds; selanyltriazoles; selenium compounds
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Funding
- Coordenacao de Aperfeicoamento de Pessoal de Nivel Superior (CAPES)
- Conselho Nacional de Desenvolvimento Cientifico e Tecnologico (CNPq) [447595/2014-8, 400150/2014-0, 306430/2013-4]
- Fundacao de Amparo a Pesquisa do Estado do Rio Grande do Sul (FAPERGS)
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We describe here a simple and rapid protocol for the synthesis of (arylselanyl) phenyl-1H1,2,3-triazoles by copper-catalyzed azide-alkyne cycloaddition (CuAAC) reactions using Microwave Irradiation. The products were obtained under mild conditions in excellent yields in a short reaction time by reacting azidophenyl arylselenides with a range of terminal alkynes using catalytic amount of Cu(OAc)(2)center dot H2O/sodium ascorbate. This Click Chemistry protocol is an efficient method to synthesize new selenium compounds with potential application in biological studies and materials sciences.
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