Journal
CHEMISTRY LETTERS
Volume 46, Issue 1, Pages 45-47Publisher
CHEMICAL SOC JAPAN
DOI: 10.1246/cl.160821
Keywords
C-H functionalization; Palladium; Nitrone
Categories
Funding
- Japan Society for the Promotion of Science
- Kanazawa University SAKIGAKE Project
- Kanazawa University CHOZEN Project
- Grants-in-Aid for Scientific Research [15K17820, 17K05778] Funding Source: KAKEN
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Palladium-catalyzed C-H alkenylation of C-aryl N-t-butyl nitrones with ethyl acrylate produced ortho-alkenylated benzamide derivatives via isomerization of the nitrone moiety. The use of 1,1,1,3,3,3-hexafluoro-2-propanol/acetic acid as a solvent resulted in effective C-H alkenylation, while competitive 1,3-dipolar cycloaddition was completely suppressed.
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