Journal
CHEMICAL COMMUNICATIONS
Volume 53, Issue 2, Pages 348-351Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c6cc08891k
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Funding
- Regione Puglia: Reti di Laboratori pubblici di ricerca'' [20, 68]
- MIUR [PONa300369]
- University of Bari
- Royal Society
- Eli Lilly
- EPSRC [EP/J001538/1] Funding Source: UKRI
- Engineering and Physical Sciences Research Council [EP/K503733/1, 1648186, EP/J001538/1] Funding Source: researchfish
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Direct synthesis of NH-sulfoximines from sulfides has been achieved through O and NH transfer in the same reaction, occurring with complete selectivity. The reaction ismediated by bisacetoxyiodobenzene under simple conditions and employs inexpensive N-sources. Preliminary studies indicate that NH-transfer is likely to be first, followed by oxidation, but the reaction proceeds successfully in either order. A wide range of functional groups and biologically relevant compounds are tolerated. The use of (AcONH4)-N-15 affords N-15-labeled compounds.
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