Journal
CHEMICAL COMMUNICATIONS
Volume 53, Issue 12, Pages 2064-2067Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c6cc09940h
Keywords
-
Categories
Funding
- Conseil Regional de Normandie, CNRS
- Normandie Universite, Labex Synorg [ANR-11-LABX-0029]
- European FEDER
Ask authors/readers for more resources
We report a new procedure for the preparation of NH-sulfoximines from sulfides using PIDA as an oxidant and ammonium carbamate as the ammonia source. Excellent yields were obtained with a wide range of sulfides. The formation of acetoxy-and methoxy- lambda(6) sulfanenitrile as intermediates was proposed, both of which were converted to the NH-sulfoximine by the action of the solvent. The structure of these intermediates was confirmed by H-1,C-13 and N-15 NMR and HRMS analysis.
Authors
I am an author on this paper
Click your name to claim this paper and add it to your profile.
Reviews
Recommended
No Data Available