Journal
TOXINS
Volume 9, Issue 2, Pages -Publisher
MDPI
DOI: 10.3390/toxins9020059
Keywords
baby-food; durum wheat pasta; multi-residual method; HRMS-orbitrap
Categories
Funding
- Economy and Competitiveness Spanish Ministry [AGL2013/43194/P]
- Universitat de Valencia [OTR2013-11518INVES/CPI-16-143/APOTIP 2016-A-040]
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A simple and rapid multi-mycotoxin method for the determination of 17 mycotoxins simultaneously is described in the present survey on durum and soft wheat pasta samples. Mycotoxins included in the study were those mainly reported in cereal samples: ochratoxin-A (OTA), aflatoxin B-1 (AFB(1)), zearalenone (ZON), deoxynivalenol (DON), 3-and 15-acetyl-deoxynivalenol (3-AcDON and 15-AcDON), nivalenol (NIV), neosolaniol (NEO), fusarenon-X, (FUS-X), T-2 toxin (T-2) and HT-2 toxin (HT-2), fumonisin B-1 and B-2 (FB1 and FB2), and four emerging mycotoxins: three enniatins (ENA, ENA(1), and ENB), and beauvericin (BEA). Twenty-nine samples were analyzed to provide an overview on mycotoxin presence: 27 samples of durum wheat pasta, and two samples of baby food. Analytical results concluded that trichothecenes showed the highest incidence, mainly DON, NIV, and HT-2 toxin, followed by ZON and ENB, while NEO, FUS-X, OTA, AFB(1), and FUM were not detected in any sample. The highest contents corresponded to ENB and ranged from 91.15 mu g/kg to 710.90 mu g/kg.
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