Journal
CHEMICAL COMMUNICATIONS
Volume 53, Issue 26, Pages 3757-3760Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c7cc00635g
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Funding
- Intramural Project CIBER-BBN ORDECA''
- DGI Grants [CTQ2013-40480-R, MAT2016-80826-R, BIO2013-45793-R, BIO2016-78006-R]
- AGAUR Grant [2014SGR-0017]
- Spanish MINECO through the Severo Ochoa Centres of Excellence Programme Grant [SEV-2015-0496]
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Herein, we report the synthesis and the study of a novel mixed biradical with BDPA and TEMPO radical units that are covalently bound by an ester group (BDPAesterTEMPO) as a polarizing agent for fast dissolution DNP. The biradical exhibits an extremely high DNP NMR enhancement of > 50000 times, which constitutes one of the largest signal enhancements observed so far, to the best of our knowledge.
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