Journal
EUROPEAN JOURNAL OF ORGANIC CHEMISTRY
Volume 2015, Issue 30, Pages 6602-6605Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/ejoc.201501075
Keywords
C-H activation; Rhodium; Dehydrogenation; Deoxygenation; Sulfur heterocycles
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Funding
- National Natural Science Foundation of China (NSFC) [21103022]
- Foundation of Fujian Educational Committee [JK2014010]
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A novel strategy for the synthesis of dibenzothiophene derivatives is established through a one-pot intramolecular cross-dehydrogenative-coupling reaction of diaryl sulfoxides followed by deoxygenation with a Rh/Ag catalytic system. The yields obtained were good to excellent (up to 96%), therefore making the described protocol an attractive option for building dibenzothiophene compounds.
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