Journal
EUROPEAN JOURNAL OF ORGANIC CHEMISTRY
Volume 2015, Issue 8, Pages 1727-1734Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/ejoc.201500006
Keywords
Synthetic methods; Photochemistry; C-H heteroarylation; Cross-coupling; Heterocycles; Radical reactions
Categories
Funding
- Department of Science and Technology (DST), New Delhi [SR/S2/JCB-11/2008]
- Indian National Science Academy, New Delhi
- Council of Scientific and Industrial Research (CSIR), New Delhi
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An efficient C-H heteroarylation of heteroarenes is achieved through visible-light photoredox-catalyzed diazotization of heteroarylamines in situ by tBuONO at room temperature. A library of functionalized biheteroaryls is obtained by using this protocol. The reaction avoids the use of transition-metal catalysts, additives, and acidic reaction medium.
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