Journal
CHEMCATCHEM
Volume 9, Issue 7, Pages 1177-1181Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/cctc.201601654
Keywords
cycloadditions; heterogeneous catalysis; mcm-41; photocatalysis; sustainable chemistry
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Funding
- Czech Science Foundation [14-09190S]
- Czech Ministry of Education, Youth and Sports [LO1201]
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7,8-Dimethoxy-3-methylalloxazine was immobilized on mesoporous silica (MCM-41) to provide a heterogenized flavin photocatalyst. Thus, the prepared heterogeneous catalyst 2 was found to sensitize the visible light [2+2] cycloaddition of various types of dienes to produce corresponding cyclobutanes in high yields and diastereoselectivities. Use of 2 enables procedures which are advantageous owing to simple operation and workup, no additives required, and minimum waste generation.
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