Journal
EUROPEAN JOURNAL OF ORGANIC CHEMISTRY
Volume 2015, Issue 5, Pages 933-937Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/ejoc.201403542
Keywords
Electrochemistry; Energy storage; Batteries; Lithium; Sulfur; Heterocycles
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Funding
- Federal Ministry of Education and Research (BMBF, HE-Lion) [03X4612B]
- German Research Foundation (DFG) in the frame of the research unit [FOR1616]
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Naphthyridines have been identified as structural elements in sulfurized polyacrylonitrile, which is a common electrode material in lithium-sulfur batteries. Some dibenzonaphthyridine derivatives with a fused dithiolo moiety were prepared as model compounds for battery studies. These heterocyclic systems were prepared via the corresponding diphenyldicarbamide intermediate. Followed by naphthyridione formation, stepwise installation of the dithiolane subunit occurred in a straightforward manner. In the solid state, the heteroaromatic system is completely planar and was thoroughly characterized. Initial battery cycling tests indicated a potential use of such structural motifs in sulfur-lithium systems.
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