Journal
ANALYTICAL CHEMISTRY
Volume 89, Issue 6, Pages 3266-3271Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.analchem.7b00142
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Funding
- Deutsche Forschungsgemeinschaft (DFG)
- Studienstiftung des Deutschen Volkes
- Arbeitsgemeinschaft industrieller Forschung (AiF)
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Utilizing temperature as an active parameter for optimization in chip-based liquid chromatography is an important step toward high-speed and high-efficiency separations on the microscale. A device including a low thermal mass micro thermostat and a microfluidic glass chip as central elements were designed and evaluated for maximal heating performance of up to 4.7 C-omicron s(-1) at up to 200 C-omicron. With this enabling technology, high-speed separations in temperature gradient mode were performed both in common reversed-phase eluents and environmental friendly ethanol-based alternatives.
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