Journal
ANGEWANDTE CHEMIE-INTERNATIONAL EDITION
Volume 56, Issue 21, Pages 5912-5915Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/anie.201702511
Keywords
aerobic oxidation; benzaldehydes; catalysis; C-H activation; solvent effects
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Funding
- Israel Ministry of Science, Technology and Space [3-10855]
- Israel Science Foundation [164/16]
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Efficient and highly selective catalytic conditions for the aerobic autoxidation of methylarenes to benzaldehydes, based on N-hydroxyphthalimide (NHPI) and cobalt(II) acetate in 1,1,1,3,3,3-hexafluoropropan-2-ol (HFIP), were developed. The sustainable conditions enable a multigram scale preparation of benzaldehyde derivatives in high efficiency and with excellent chemoselectivity (up to 99% conversion and 98% selectivity).
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