Journal
APPLIED SURFACE SCIENCE
Volume 404, Issue -, Pages 263-267Publisher
ELSEVIER
DOI: 10.1016/j.apsusc.2017.01.271
Keywords
Metal-organic frameworks; NMR spectroscopy; IR spectroscopy
Categories
Funding
- CSIR [HTC066P]
- South African National Research Foundation [HTC063X, HTC059X]
- National Natural Science Foundation of China [21602135]
- South African Department of Science and Technology [HTC004X]
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The in-situ IR technique was employed to monitor the crystallization process of Zr-fumarate (Zr-fum) MOF under real synthesis conditions. The results evidenced the participations of both modulator acid (HCOOH) and solvent (DMF) during the structural formation of Zr-fum MOF. This observation will contribute to the quest for understanding of the formation of structural defects in MOFs, which is a topic that is currently under intense investigation. (C) 2017 Elsevier B.V. All rights reserved.
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