Journal
ACTA MATERIALIA
Volume 130, Issue -, Pages 83-93Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.actamat.2017.03.031
Keywords
Single-source-precursor; Ceramic nanocomposite; RGO/CNTs hybrids; Dielectric properties; Electromagnetic shielding
Funding
- Natural Science Foundation of Fujian Province of China [2015J01221]
- China Scholarship Council (CSC) [201406290019]
- Japan through JSPS Bilateral Program
- Germany through JSPS Bilateral Program
- Exploratory Research program of MEXT
- Core-to-Core Program of JSPS
- Grants-in-Aid for Scientific Research [17H06094, 25106003, 17K18974] Funding Source: KAKEN
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For the first time, single-source-precursors (SSPs) were synthesized through chemical modification of a commercial poly(methylvinyl)silazane with chemically bonded graphene oxide and carbon nanotube hybrids (GO/CNTs). After pyrolysis of warm-pressed and consolidated SSP-powders at 1000 degrees C in Ar, monolithic SiCN ceramic nanocomposites modified with in-situ thermally reduced GO/CNTs, namely RGO/CNTs-SiCN, were successfully obtained. The SSP-derived nanocomposite exhibits significantly enhanced dielectric properties if compared with that of a physically-blended-precursor derived reference material. Moreover, the SSP-derived RGO/CNTs-SiCN composite containing 15.0 wt% GO/CNTs in the feed possesses an electromagnetic shielding effectiveness of 67.2 dB with a sample thickness of 2.00 mm, which is the highest value among all the reported graphene-based composites with comparable thickness. (C) 2017 Acta Materialia Inc. Published by Elsevier Ltd. All rights reserved.
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