Journal
CERAMICS INTERNATIONAL
Volume 43, Issue 9, Pages 6967-6975Publisher
ELSEVIER SCI LTD
DOI: 10.1016/j.ceramint.2017.02.121
Keywords
Fracture; Micromechanics; Ceramics; Voronoi tessellation; Finite element model
Categories
Funding
- Nanyang Technological University (NTU)
- NTU Research Student Scholarship
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The mechanisms of fracture in polycrystalline alumina were investigated at the grain level using both the micromechanical tests and finite element (FE) model. First, the bending experiments were performed on the alumina microcantilever beams with a controlled displacement rate of 10 nm s(-1) at the free end; it was observed that the intergranular fracture dominates the failure process. The full scale 3D Voronoi cell FE model of the microcantilever bending tests was then developed and experimentally validated to provide the insight into the cracking mechanisms in the intergranular fracture. It was found that the crystalline morphology and orientation of grains have a significant impact on the localised stress in polycrystalline alumina. The interaction of adjacent grains as well as their different orientations determines the localised tensile and shear stress state in grain boundaries. In the intergranular fracture process, the crack formation and propagation are predominantly governed by tensile opening (mode I) and shear sliding (mode II) along grain boundaries. Additionally, the parametric FE predictions reveal that the bulk failure load of the alumina microcantilever increases with the cohesive strength and total fracture energy of grain boundaries.
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