Journal
ACTA MATERIALIA
Volume 131, Issue -, Pages 323-335Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.actamat.2017.03.069
Keywords
High-entropy alloy; Dual phase; Phase transformations; Grain refining; Mechanical properties
Funding
- European Research Council under the EU's 7th Framework Programme (FP7)/ERC grant [290998]
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We present a systematic microstructure oriented mechanical property investigation for a newly developed class of transformation-induced plasticity-assisted dual-phase high-entropy alloys (TRIP-DP-HEAs) with varying grain sizes and phase fractions. The DP-HEAs in both, as-homogenized and recrystallized states consist of a face-centered cubic (FCC) matrix containing a high-density of stacking faults and a laminate hexagonal close-packed (HCP) phase. No elemental segregation was observed in grain interiors or at interfaces even down to near-atomic resolution, as confirmed by energy-dispersive X-ray spectroscopy and atom probe tomography. The strength-ductility combinations of the recrystallized DP-HEAs (Fe50Mn30Co10Cr10) with varying FCC grain sizes and HCP phase fractions prior to deformation are superior to those of the recrystallized equiatomic single-phase Cantor reference HEA (Fe20Mn20Ni20-Co20Cr20). The multiple deformation micro-mechanisms (including strain-induced transformation from FCC to HCP phase) and dynamic strain partitioning behavior among the two phases are revealed in detail. Both, strength and ductility of the DP-HEAs increase with decreasing the average FCC matrix grain size and increasing the HCP phase fraction prior to loading (in the range of 10-35%) due to the resulting enhanced stability of the FCC matrix. These insights are used to project some future directions for designing advanced TRIP-HEAs through the adjustment of the matrix phase's stability by alloy tuning and grain size effects. (C) 2017 Acta Materialia Inc. Published by Elsevier Ltd. All rights reserved.
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