Journal
RSC ADVANCES
Volume 7, Issue 74, Pages 46704-46712Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c7ra07128k
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- Ministry of Science and Technology of the Republic of China [MOST 103-2113-M-003-008-MY3]
- National Taiwan Normal University [103-07-C]
- Instrumentation Centre at National Taiwan Normal University
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An approach for the synthesis of functionalized unsymmetrical 1,3-butadiene-3-yne derivatives is reported starting from beta-halo styrene and phenyl acetylene derivatives in the presence of PdCl2 and CuI catalysts. Functional groups such as aldehyde, cyano and ester groups are well tolerated and afford the desired functionalized dienynes. Further, these 1,3-buta-diene-3-yne derivatives are utilized for the synthesis of novel trisubstituted pyridine derivatives.
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