Journal
RSC ADVANCES
Volume 7, Issue 66, Pages 41755-41762Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c7ra08637g
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Funding
- Department of Science and Technology, New Delhi, India [SR/S2/JCB26/2010]
- Council of Scientific and Industrial Research, New Delhi
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Glycals were found to react with a reagent system comprising of phenyliodine bis(trifluoroacetate) (PIFA) and Me3SiN3 in the presence of TMSOTf as a catalyst to form the corresponding vicinal 1,2-diazides. On the other hand, they reacted with another reagent system phenyliodine diacetate (PIDA) and Me3SiN3, also in the presence of TMSOTf as a catalyst, to lead to the corresponding vicinal 1,2-azidoacetates. These azido derivatives were converted into a number of 2-azido-N-glycopeptides, pseudotrisaccharides, and a piperidine triol derivative, an iminosugar.
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