Journal
CATALYSIS SCIENCE & TECHNOLOGY
Volume 7, Issue 11, Pages 2165-2169Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c7cy00336f
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Funding
- U.S. Department of Energy, Office of Science, Office of Basic Energy Sciences [DOE DE-FG02-03ER154757]
- National Science Foundation [NSF CHE-9871268, NSF CHE-1048773, NSF DMR-0521267, CHE-1213235]
- Soft and Hybrid Nanotechnology Experimental (SHyNE) Resource [NSF NNCI-1542205]
- MRSEC program at the Northwestern Materials Research Center [NSF DMR-1121262]
- International Institute for Nanotechnology (IIN)
- Keck Foundation
- State of Illinois, through the IIN
- Direct For Mathematical & Physical Scien
- Division Of Chemistry [1464488] Funding Source: National Science Foundation
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Reductive coupling of various carbonyl compounds to the corresponding symmetric ethers with dimethylphenylsilane is reported using a carbon-supported dioxo-molybdenum catalyst. The catalyst is air- and moisture-stable and can be easily separated from the reaction mixture for recycling. In addition, the catalyst is chemoselective, thus enabling the synthesis of functionalized ethers without requiring sacrificial ligands or protecting groups.
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