Journal
ACS CATALYSIS
Volume 7, Issue 8, Pages 4986-4989Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acscatal.7b01535
Keywords
redox organocatalyst; flavin; iodine; aerobic oxidation; thiadiazole
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Funding
- JSPS/MEXT KAKENHI [16K05797, 26105724]
- Sumitomo Foundation
- Cooperative Research Program of the Institute for Protein Research, Osaka University [CR-16-05]
- Grants-in-Aid for Scientific Research [26105724, 16K05797] Funding Source: KAKEN
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A bioinspired two-component redox organocatalyst system using 1,10-bridged flavinium and NH4I was developed to perform environmentally friendly aerobic oxidative ring formation of 1,2,3-thiadiazoles from N-tosylhydrazones and sulfur. The redox organocatalysis of the flavinium promoted the iodine-catalyzed system without the use of any sacrificial reagents, except for environmentally benign molecular oxygen.
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