4.7 Article

Ultraclean pure shift NMR

Journal

CHEMICAL COMMUNICATIONS
Volume 53, Issue 73, Pages 10188-10191

Publisher

ROYAL SOC CHEMISTRY
DOI: 10.1039/c7cc04423b

Keywords

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Funding

  1. AstraZeneca
  2. Engineering and Physical Sciences Research Council [EP/M013820, EP/N033949]
  3. Engineering and Physical Sciences Research Council [EP/L018500/1, EP/N033949/1] Funding Source: researchfish
  4. EPSRC [EP/N033949/1, EP/L018500/1] Funding Source: UKRI

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Pure shift'' methods can greatly improve the resolution of proton NMR spectra. However, current pure shift spectra show small periodic artefacts that prevent their use for studying dilute mixture components. A new technique, compatible with all current pure shift methods, is presented that suppresses such sidebands to arbitrary order, allowing ultraclean spectra to be obtained.

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