4.1 Article

Crystal structure of di-μ-chlorido-bis[1,2-bis(dicyclohexylphosphino)-1,2-dicarba-closo-dodecaborane-κ2P,P′] zinc(II), C52H108B20Cl2P4Zn2

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WALTER DE GRUYTER GMBH
DOI: 10.1515/ncrs-2016-0155

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Funding

  1. Key Scientific Research Projects of Colleges and Universities, Henan Province [16A150001, 16A430012]
  2. Research Fund of Anyang Institute of Technology [YJJ2015021, YJJ2015022]

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C52H108B20Cl2P4Zn2, monoclinic, C2/c (no. 15), a = 31.783(3) angstrom, b = 10.0780(10) angstrom, c = 24.9326(19) angstrom, beta = 109.901(2)degrees, V = 7509.2(11) angstrom(3), Z = 4, R-gt(F) = 0.0569, wR(ref)(F-2) = 0.0972, T = 298 K. CCDC no.: 1504437 The crystal structure is shown in the figure. Tables 1 and 2 contain details of the measurement method and a list of the atoms including atomic coordinates and displacement parameters.

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