Journal
APPLIED SURFACE SCIENCE
Volume 421, Issue -, Pages 453-459Publisher
ELSEVIER SCIENCE BV
DOI: 10.1016/j.apsusc.2016.09.106
Keywords
Ellipsometry; Inversion; Optical constants; Dielectric function; Thin films; Optical properties; ZnO
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An original method of ellipsometric data inversion is proposed based on the use of constrained splines. The imaginary part of the dielectric function is represented by a series of splines, constructed with particular constraints on slopes at the node boundaries to avoid well-know oscillations of natural splines. The nodes are used as fit parameters. The real part is calculated using Kramers-Kronig relations. The inversion can be performed in successive inversion steps with increasing resolution. This method is used to characterize thin zinc oxide layers obtained by a sol-gel and spin-coating process, with a particular recipe yielding very thin layers presenting nano-porosity. Such layers have particular optical properties correlated with thickness, morphological and structural properties. The use of the constrained spline method is particularly efficient for such materials which may not be easily represented by standard dielectric function models. (C) 2016 Elsevier B.V. All rights reserved.
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