Journal
CHEMICAL COMMUNICATIONS
Volume 53, Issue 69, Pages 9606-9609Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c7cc04348a
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Funding
- Natural Science and Engineering Research Council of Canada (NSERC) [RGPIN-06438]
- Canada Foundation for Innovation Leaders Opportunity Funds [227346]
- Canada Research Chair Program [CRC-227346]
- FRQNT Team Grant [PR-190452]
- FRQNT Centre in Green Chemistry and Catalysis (CGCC) Strategic Cluster [RS-171310]
- Universitede Montreal
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Herein is described an improved synthetic route to enantio- and diastereoenriched iodocyclopropylmethanols using (diiodomethyl)zinc iodide etherate as the active species. The products obtained by this methodology were successfully functionalized by SuzukiMiyaura cross-coupling reactions. A Buchwald-type palladium precatalyst allowed access to highly substituted and stereo-enriched cyclopropanes without requiring a protecting group.
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