Journal
ULTRASONICS SONOCHEMISTRY
Volume 39, Issue -, Pages 534-539Publisher
ELSEVIER
DOI: 10.1016/j.ultsonch.2017.05.031
Keywords
Ultrasonic irradiation; Green sonochemical protocol; Magnetic core/shell nanocatalyst; Nitration; Deep eutectic solvent
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Funding
- Iran National Science Foundation (INSF)
- Research Council of the Iran University of Science and Technology (IUST)
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An efficient sonochemical protocol for the nitration of aromatic compounds was described in the presence of a catalytic amount of sulfuric acid-functionalized silica-based core/shell magnetic nanocomposite at room temperature in an eco-friendly and recyclable media, deep eutectic solvent (DES), based on choline chloride and urea. The particle size, morphology and elemental analysis of the core/shell nanocatalyst were carried out by TEM, SEM, EDX and XRD analyses. The nanocatalyst and DES were easily recovered from the reaction mixture quantitatively and reused several times.
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