Journal
CHEMICAL COMMUNICATIONS
Volume 53, Issue 96, Pages 12886-12889Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c7cc07483b
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Funding
- Ministry of Science and Technology of the People's Republic of China [2016YFA0501203]
- National Natural Science Foundation of China [31470727, 21475004]
- Beijing National Laboratory for Molecular Sciences
- 1000 Plan Program for Young Talents of China
- NWO VENI [722.016.002]
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We report a novel proton-detected MAS solid-state NMR strategy based on N-15-N-15 proton assisted recoupling to detect the inter-nucleotide NH center dot center dot center dot N hydrogen bonds within the Watson-Crick base pairs of micro-crystallized dimeric RNA and to confirm the kissing-loop structure. This would contribute to advances in the structural determination of RNA using solid-state NMR.
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