Journal
TETRAHEDRON
Volume 73, Issue 38, Pages 5599-5604Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tet.2017.02.056
Keywords
Furfural conversion; Flow chemistry; Pd; Nanoparticles; Hydrogenation; Heterogeneous catalysis
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Funding
- Consejeria de Ciencia e Innovacion, Junta de Andalucia [P10-FQM-6711]
- COST Action under STSM at group of C.L. in UTC [FP1306, COST-STSM-FP1306-33358]
- Sorbonne Universities at UTC
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A number of synthesized supported Pd nanomaterials on aluminosilicate supports were investigated in the continuous flow hydroconversion of furfural to a range of furanic derivatives as compared to a commercial Pd/C catalyst. Excellent furfural conversions (>60%) and varying selectivities to products at mild temperatures (90 degrees C) could be obtained for most catalytic systems, with interesting selectivities to furfuryl alcohol (FOL), 2-methylfuran (MF) and tetrahydrofurfuryl alcohol (THFOL) depending on type of Pd catalyst. A significant deactivation with time on stream was observed for continuous flow synthesized nanomaterials with respect to commercial 5%Pd/C. (C) 2017 Elsevier Ltd. All rights reserved.
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