Journal
TETRAHEDRON
Volume 73, Issue 49, Pages 6954-6961Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tet.2017.10.057
Keywords
Phenols; Nanocomposite; Hydrolysis; Aryldiazonium silica sulfate; Solvent-free conditions
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Funding
- Islamic Azad University, Fasa Branch and Khorasgan Branch
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The hydrolysis of a new type of diazonium salt immobilized on the surface of silica sulfuric acid was studied in this work. By using diazonium salt nanocomposites, a number of phenol derivatives were synthesized in good yields. In contrast to the previous works, the present procedure was conveniently carried out under mild and solvent-free conditions. The effects of solvent and temperature were studied on the dediazoniation products. The notable advantages of this methodology were operational simplicity, availability of reactants, short reaction time and easy work-up. (C) 2017 Elsevier Ltd. All rights reserved.
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