Journal
SYNTHESIS-STUTTGART
Volume 50, Issue 5, Pages 1141-1151Publisher
GEORG THIEME VERLAG KG
DOI: 10.1055/s-0036-1591842
Keywords
isothiocyanates; desulfuration; propane phosphonic acid anhydride (T3P (R)); dithiocarbamates; amino acids; amines
Categories
Funding
- Polish National Science Centre [DEC 2011/03/B/ST5/01058]
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A number of alkyl, aryl and bifunctional isothiocyanates are obtained in moderate to high yields (41-94%) in a two-step, one-pot reaction of the parent primary amines or their salts with carbon disulfide, followed by reaction of the thus formed dithiocarbamates with T3P (R) (propane phosphonic acid anhydride) as a new and efficient desulfurating agent.
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