Journal
SYNLETT
Volume 28, Issue 13, Pages 1586-1591Publisher
GEORG THIEME VERLAG KG
DOI: 10.1055/s-0036-1588806
Keywords
nickel; DPEPhos; C-N cross-coupling; anilines; secondary amines; azoles
Categories
Funding
- Natural Sciences and Engineering Research Council of Canada [RGPIN-2014-04807]
- Natural Sciences and Engineering Research Council of Canada (I2I) [I2IPJ/485197-2015]
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Synthesis and characterization of the new air-stable pre-catalyst (DPEPhos)Ni(2-mesityl)Br (C1) is reported, along with the application of this pre-catalyst in the cross-coupling of secondary amines/azoles with activated (hetero) aryl chlorides to afford tertiary (hetero) anilines. The performance of C1 in these cross-couplings is competitive with some of the best and/or most widely employed nickel catalysts for such transformations.
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