Journal
SYNLETT
Volume 29, Issue 1, Pages 46-50Publisher
GEORG THIEME VERLAG KG
DOI: 10.1055/s-0036-1590922
Keywords
radical; fluorine; alkenes; elimination; enols; allylation; xanthate
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Funding
- excellence laboratory LabEx SYNORG [ANR-11-LABX-0029]
- Conseil Regional de Normandie
- European FEDER fundings
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Triethylborane-mediated radical allylation was performed from Morita-Baylis-Hillman alcohols with no need of protecting group. The radical conjugated addition-elimination reaction is highly selective, and trisubstituted E-alkenes were obtained. This reaction opened a new route for the preparation of functionalized ,-unsaturated ketones.
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