Journal
SYNLETT
Volume 28, Issue 19, Pages 2619-2623Publisher
GEORG THIEME VERLAG KG
DOI: 10.1055/s-0036-1589082
Keywords
phenols; styrenes; cyclization; oxidation; dihydrobenzofurans
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Funding
- Open Foundation of Key Laboratory of Synthetic and Natural Functional Molecule Chemistry of the Ministry of Education of China
- Science and Technology Program of Xi'an City
- Shaanxi Province [2017KW-066]
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A catalyst-free oxidative [3+2] cycloaddition of phenols and styrenes was developed with 2,3-dichloro-5,6-dicyano-1,4-benzoquinone as the oxidant and 1,1,1,3,3,3-hexafluoropropan-2-ol as the solvent at room temperature. With this method, a broad range of dihydrobenzofurans were efficiently and quickly obtained from readily available phenols and styrenes.
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