Journal
MOLBANK
Volume -, Issue 4, Pages -Publisher
MDPI
DOI: 10.3390/M960
Keywords
quinoline; amide; chalcone
Categories
Funding
- FONDECYT [1150712]
- PIEI QUIMBIO, project, Utalca
- Scholarship CONICYT [63140046]
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An amide chalconehas been synthesized in a two-step reaction. First, N-(4-acetylphenyl) quinoline-3-carboxamide 2 was synthesized by the reaction of quinoline-3-carboxylic acid 1 and thionyl chloride (SOCl2), following the addition of 4-aminoacetophenone. Then, a typical Claisen-Schmidtreactionwas made between 2 and piperonal using KOH solution as a catalystin ethanol, under ultrasonic irradiation. The structure of the target compound was established by FTIR (Fourier-transform infrared spectroscopy), HRMS, H-1 and C-13-NMR.
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