Journal
ADVANCED SYNTHESIS & CATALYSIS
Volume 360, Issue 2, Pages 284-289Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/adsc.201701143
Keywords
Nickelacycle; annulation; benzyne; nickel; phenanthridinone
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Funding
- Ministry of Science and Technology of the Republic of China [MOST 103-2633-M-007-001]
- Ministry of Education for Taiwan Government
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The synthesis of phenanthridinones via denitrogenative annulation of 1,2,3-benzotriazin-4-(3H)-ones with arynes catalysed by Ni(0)/dppm was successfully developed. A variety of phenanthridinones were prepared in good to excellent yields. Based on this method, nature product, N-methylcrinasidine, was synthesized.
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