Journal
RUSSIAN JOURNAL OF GENERAL CHEMISTRY
Volume 87, Issue 5, Pages 1064-1072Publisher
MAIK NAUKA/INTERPERIODICA/SPRINGER
DOI: 10.1134/S1070363217050280
Keywords
triethanolamine; 2-amino-4H-chromenes; transition metal-free catalysis; green chemistry; electrosynthesis
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Funding
- Research Council of Hakim Sabzevari University
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A wide variety of 2-amino-4H-chromene derivatives with diverse substituents on the 4H-chromene ring were efficiently prepared via one-pot three-component reaction of an aromatic aldehyde and malononitrile with 2-hydroxynaphthalene-1,4-dione, ethyl acetoacetate, or naphthols in the presence of triethanolamine as a new organocatalyst under solvent-free conditions. The procedure is transition metal-free and environmentally friendly approach to various 2-amino-4H-chromene derivatives. Its advantages include short reaction time, high yields, low cost, and straightforward work-up. Triethanolamine is an efficient reusable catalyst. 2-Amino-4H-benzo[g]chromenes (ABgC) were applied as novel components of electro synthesis of silver nanoparticles.
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