Journal
ARKIVOC
Volume -, Issue -, Pages 149-157Publisher
ARKAT USA INC
DOI: 10.24820/ark.5550190.p010.497
Keywords
Michael-type addition; microwave assisted; bismuth triflate; 1-(arylsulfonyl)pyrroles; 1-(phenylsulfonyl)indoles
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Funding
- National Science Foundation - Course, Curriculum, and Laboratory Improvement (CCLI) Instructional Materials Development, Procter & Gamble Fund, Curriculum Development Grant for Rapid Transfer of Knowledge and Technology [DUE-0127240]
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The Michael type addition of pyrroles and indoles bearing strongly electron-withdrawing N-protecting groups (e.g., arylsulfonyl-, benzoyl-) to methyl vinyl ketone have not been previously reported. We find that such alkylative processes can be effected in low to moderate yields using bismuth triflate as catalyst in conjunction with microwave irradiation. [GRAPHICS] .
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